@All
I do appreciate all your help and comments and I have no intention of going down without a fight. I have no real choice than to wait until Christmas to find out what the material is and then rewrite. I will use the time producing another 2 papers, which don't rely on the XRD and I had planned an extended literature review to be published separately.
My papers and thesis will have to wait until the data is available and I will have to apply for an extension, which they will have to give me or I really will document all the things my supervisor has done over the last 4 years, send it to the sponsors and to hell with it!
If it takes me another year, it may not look good on my CV, but at least I will have good papers which will hopefully secure me a good post-doc.
I'm quite shocked that a supervisor would say 'everybody does it' in relation to false data! There's a big difference between some undergrads replicating an experiment that's been done 20,000 times already and someone who's actually got a career based on being at the forefront of scientific knowledge. It is a shame we have such a results-driven academic culture in some ways - the studies that show strange, confusing or disappointing results are just as valid as the ones with the big breakthroughs!
Good luck with sorting things out, Albatross1986.
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